| Preface / S. Szymanski |
| Proton Tunnelling |
| Effects in Metal Hydride NMR / N. Asakawa ; T. Kameda ; S. Kuroki ; H. Kurosu ; S. Ando ; I. Ando ; A. Shoji |
| Structural Studies of Hydrogen-Bonded Peptides and Polypeptides by Solid State NMR / W.S. Price |
| NMR Imaging / J. Grandjean |
| NMR Studies of Interfacial Phenomena |
| Subject Index |
| (Chapter Headings) Application of NMR Spectroscopy to Sciences and Technologies of Glasses and Ceramics / C. Faber ; W.P. Power |
| Applications of NMR to Food Science |
| Application of 207PB NMR Parameters / Keith Orrell ; J.C. Lindon |
| High-Resolution Solid State NMR Studies on Ceramics / 1： |
| Gradient NMR |
| Dynamic aspects of membrane proteins and membrane-associated |
| In vivo Proton NMR Studies in Skeletal Musculature |
| Applications of Heteronuclear X,Y-Correlation |
| Applications of 29 Si NMR Parameters |
| Advances in Probe Design for Protein NMR |
| Resolution enhancement in in vivo NMR spectroscopy / P.D. Ellis |
| NMR Studies of Zeolites / R.E. Wasylishen |
| Pharmaceutical Applications of NMR |
| Dynamic NMR Spectroscopy Inorganic and Organometallic Chemistry |
| Peptides as revealed by 13C NMR: lessons from bacteriorhodopsin as an intact protein / J.K. Nicholson |
| Quality Assessment of Horticultural Products by NMR |
| Spectroscopy in Organometallic and Organoelement Chemistry |
| NMR Studies of Higher-Order Structures of Solid Polymers / F. Stallmach2： |
| Nuclear Magnetic Resonance Spectroscopy in Forensic Science |
| Applications of NMR to food science / A. M. Gil |
| Applications of NMR to Thermostable Proteins |
| Applications of NMR in Solid-Phase Synthesis |
| NMR Studies of b-type Haemoproteins Reconstituted with a Ring-Fluorinated Haem |
| Diffusion in Soft Polymer Systems as Approached by Field Gradient NMR |
| Organic Thin Films / A.S. Lipton ; R.G. Kidd |
| NMR of persistent carbocations from ploycyclic aromatice hydrocarbons(PAHS) / J.R. Everett |
| High Pressure NMR Studies on Lyotropic Lipid Mesophases and Model Biomembranes |
| Advances in Theoretical and Physical Aspects of Spin-Spin Couplings |
| Diffusion in a closed sphere / P. Galvosas ; C. Pascoal Neto3： |
| A Study of Conformational Stability of Polypeptide Blends by Solid State NMR Spectroscopy |
| Site Directed Solid State NMR on Membrane Proteins |
| How Far Can the Sensitivity of NMR be Increased? |
| Low Temperature Solid-State NMR Spectroscopy. A Strategy for the Direct Observation of Quadrupolar Nuclides of Biological Interest |
| NMR Studies of Isolated Spin Pairs in the Solid State |
| NMR Spectroscopy of Biofluids |
| Automatic Analysis of NMR Spectra |
| Spin echo NMR direg;usion studies / 4： |
| Solid State NMR Studies of Wood and other Ligno-Cellulose Materials / B.E. Mann |
| High Pressure NMR Studies in Proteins / J.F. Hinton |
| Applications of Low-Field NMR to Food Science |
| The Oxidation-State Dependence of Transition-Metal Shieldings / D.A. Middleton ; L.B. Krivdin ; Brian J. Goodfellow5： |
| NMR Studies of Ion Transporting Biological Channels |
| Xenon NMR Spectroscopy |
| Residual Dipolar Couplings: Measurements and Applications to Biomolecular Studies |
| NMR methods for Characterising ligand-receptor and drug-membrane interactions in pharmaceutical research |
| Recent advances in theoretical calculations of indirect spin-spin coupling constants / R.H. Contreras ; Anjos L. Macedo ; D. Gudat ; L. Ernst |
| NMR Structural Studies of Iron-Sulpher Proteins / G. Binsch |
| Applications of Heteronuclear X,Y--Correlation Spectroscopy in Organometallic and Organoelement Chemistry |
| Recent Advances in NMR Studies of Cyclophanes / Qun Chen ; Ana Ramos ; B. Wrackmeyer |
| The Cinderella Nuclei |
| Application of 119Sn NMR Parameters / Hiromichi Kurosu ; J. Kowalewski ; Helena Santos |
| Solid-state NMR studies on semicrystalline polymers / A. Iuga et al. ; J. Malito |
| Permutation Symmetry in NMR Relaxation and Exchange |
| NMR Studies of Wine Chemistry and Wine Bacteria |
| Applications of solid-state 31P NMR spectroscopy |
| Nuclear Spin Relaxation in Diamagnetic Fields / J. Farjon et al. |
| Copper-63 NMR Spectroscopy / Claudio Dalvit |
| Selective NMR excitations in chiral analysis / S.L GragePart 2： |
| Water Signal Supression in NMR Spectroscopy / W. Meiler ; J. M. Boehlen |
| Proton Phase Sensitive Pulsed-Field-Gradient Double-Quantum NMR Spectroscopy / A. Watts ; R. Meusinger, NMR of Coals and Coal Products |
| Applications of REDOR for Distance Measurements in Biological Solids / T. Baba |
| Organic Systems and Solutions of Macromolecules and Aggregates |
| Index. / Y. Ono |
| Variable Temperature 1H MAS NMR: A Powerful Tool for the Investigation of Dynamic Properties of Acidic Protons in Zeolites and Heteropoly Compounds |
| List of Contributors |
| Long-Range [superscript 1]H-[superscript 15]N Heteronuclear Shift Correlation / Gary E. Martin ; Antony J. Williams |
| Introduction |
| New Long-Range Heteronuclear Shift Correlation Methods |
| NMR Probe Technology Developments |
| Computer-Assisted Structure Elucidation Using [superscript 15]N Chemical Shift and [superscript 1]H-[superscript 15]N Long-Range Correlation Information |
| Long-Range Correlation Studies Involving [superscript 15]N |
| Conclusions / 6： |
| References |
| Magic-Angle-Spinning Solid-State NMR Applied to Polypeptides and Proteins / Colan E. Hughes ; Marc Baldus |
| Methods |
| Applications |
| Acknowledgements |
| NMR Studies of Dynamic Processes in Organic Solids / D. Reichert |
| Experimental Methods |
| Applications of Dynamic Solid-State NMR in Organic Solids |
| NMR Studies of Nanoparticles / Christian Mayer |
| Nuclear Magnetic Resonance Techniques |
| Numerical Simulation Procedure |
| General Applications and Examples |
| Conclusion |
| Microscopy in Magnetic Resonance Imaging / P.T. Narasimhan ; Russell E. Jacobs |
| Signal and Noise in Magnetic Resonance Imaging |
| Contrast |
| Imaging Methods, Pulse Sequences, and the Point Spread Function |
| Other Imaging Methods |
| Prospects for Higher Resolution / 7： |
| Applications of Optical Pumping and Polarization Techniques in NMR: I. Optical Nuclear Polarization in Molecular Crystals / Boyd M. Goodson |
| Multiple Quantum NMR of Partially Aligned Molecules / Leslie D. Field |
| NMR of partially aligned molecules |
| Multiple quantum NMR and spectral simplification |
| Excitation and detection of multiple quantum coherence |
| Selective deuteration to simplify spectral analysis |
| The analysis and simulation of multiple quantum spectra |
| Heteronuclear MQNMR |
| Measuring diffusion in anisotropic media using MQNMR / 8： |
| Multiple quantum spectra of exchanging systems / 9： |
| MQ relaxation in anisotropic media / 10： |
| Counting spins in clusters / 11： |
| Studies of aligned molecules by MQNMR / 12： |
| Solid-State NMR Studies of Molecular Motion / Melinda J. Duer |
| Lineshape analysis and measurement of motionally averaged interactions |
| Relaxation time measurements |
| Exchange experiments |
| NMR Studies of Phase Transitions / C. Odin |
| Phase Transitions and NMR: Generalities and Static Contribution |
| Phase Transitions and NMR: Motions |
| Ferroelectric Phase Transitions, H-Bonded Systems |
| Coexistence, Hysteresis and Kinetics |
| Single-Crystal Phase Transition Studies |
| Miscellaneous Phase Transitions |
| Conclusion and Perspectives |
| Acknowledgment |
| Application of Multi-Way Analysis to 2D NMR Data / Henrik T. Pedersen ; Marianne Dyrby ; Soren B. Engelsen ; Rasmus Bro |
| General theory |
| Analysis of 2D and 3D NMR data |
| High-Resolution Protein Structure Determination by NMR / Hiroyuki Takashima |
| Statistics of protein structures solved by NMR on protein data bank |
| Critical factors for NMR structure qualities |
| High-performance computing |
| NMR structure determination process overview |
| Structure calculation |
| High-performance computing implementation for structure determination |
| Basic NMR-derived constraints for structure calculations |
| Improve target function quality |
| Dynamics |
| Quality check of the NMR ensemble |
| Protein sample preparations |
| NMR Experiments / 13： |
| Concluding remarks / 14： |
| Acknowledgments |
| Index |
| Applications of NMR Spectroscopy to the Structure and Ionic Aggregates of Ionomers |
| Applications of NMR Techniques to Coal Science |
| An NMR study of strongly correlated superconductors |
| NMR in Context / P.S. Belton |
| Magnetic Resonance Imaging / M.J. McCarthy ; M.K. Cheung |
| Magnetic Resonance Microscopy / X. Zhou ; T.L. Peck ; J.B. Litchfield |
| Stable IsotopeAnalysis of Food and Beverages by Nuclear Magnetic Resonance / G.J. Martin ; M.L. Martin |
| On-line Applications in Food Science / C. Tellier ; F. Mariette |
| The Use of ESR Spectroscopy for the Identification of Irradiated Food / M.H. Stevenson ; R. Gray |
| Wide-line and High-resolution in 1H NMR of Food Materials / T.M. Eads |
| Conformational Characterization of Polysaccharides as Studied by High-resolution 13C Solid-state NMR / H. Saito |
| Studies of Protein Structure by NMR Spectroscopy / G.M. Smith |
| NMR of Lipids / F.D. Gunstone ; V.K.S. Shukla |
| Probing Water Relations in Food Using Magnetic Resonance Techniques / X. Sun ; S.J. Schmidt |
| Milk / N.M. Wahlgren ; T. Drakenberg |
| NMR Studies in Meat / J.-P. Renou |
| Applications of NMR to Drying / J.E. Maneval |
| Chapter References |
| Contributors |
| Magnetic Resonance of Systems with Equivalent Spin-1/2 Nuclides / John A. Weil |
| Preamble |
| Exchange Actions and Interactions |
| Equivalent Nuclides Within a Molecular Species |
| The Effects of Motions |
| Exchange Degeneracy |
| Spin-Spin Interactions of Sets of Distinct Particles |
| Selected Molecules with Equivalences |
| Spin-Hamiltonian Parameters |
| Spectral Degeneracy |
| Acknowledgement |
| Protein Dynamics as Reported by NMR / Zoltán Gáspári ; András Perczel |
| Motions and Time Scales in Proteins |
| Representation of Protein Structure and Dynamics |
| Exploring Protein Structure and Dynamics: A Brief Overview of Techniques |
| NMR Spectroscopy for Determining Protein Structure and Dynamics |
| Examples Highlighting the Role of Protein Internal Dynamics in Biological Processes |
| Concluding Remarks |
| Virtual MRS: Spectral Simulation and its Applications / Brian J. Soher ; Karl Young ; Lana Kaiser |
| Introduction and Background |
| From Physics to Object-Oriented Programming |
| Practical Applications and Implications |
| Simulation of Molecular Motion of Quadrupolar Nuclei in Solid-State NMR Spectra / Flemming H. Larsen |
| Theory |
| Numerical Simulations |
| Results and Discussion |
| NMR Studies of Disorder in Condensed Matter Systems / K. P. Ramesh |
| Dipolar Glasses / l： |
| NMR Study of Relaxor Ferroelectrics |
| Conducting polymers |
| Recent Advances in HMBC Studies / J. Furrer |
| Open Core NMR / K. Takeda |
| Nuclear spin relaxation for structural and stereochemical determinations in small or medium sized molecules / D.Canet |
| NMR studies on structurally or dynamically heterogeneous systems: dynamic aspects of hydrogels, protein fibrils and membrane proteins / M. Saito |
| NMR Studies of optically active Schiff bases / Z. Rozwadowski |
| Probing interactions between small molecules and polymers by means of NMR spectroscopy / M. Valentini |
| Structure and Membrane Interactions of Antimicrobial Peptides as Viewed by Solid-State NMR Spectroscopy / Marise Ouellet ; Michele Auger |
| Study of Antimicrobial Peptides in Membranes |
| Effects of Antimicrobial Peptides on Model Lipid Membranes |
| Chemical Exchange / Alex D. Bain |
| Overview, Trends and Opinions |
| Methodology |
| Conclusions and Acknowledgments |
| Rhodium-103 NMR / Laurence Carlton |
| Acquisition of Data |
| Calibration of Spectra |
| Factors Underlying the Chemical Shift |
| Influence of Temperature on the Chemical Shift |
| Influence of Solvent on the Chemical Shift |
| Other Influences on the Chemical Shift |
| Correlation of [delta]([superscript 103]Rh) with Chemical and Structural Parameters |
| Parahydrogen-Induced Polarisation (PHIP) |
| High-Pressure Studies |
| Solid-State Studies |
| Clusters |
| Calculated Chemical Shifts |
| Spin Coupling Constants |
| Relaxation Times / 15： |
| Abbreviations / 16： |
| Layout of Tables / Appendix： |
| The Indirect Detection of Metal Nuclei by Correlation Spectroscopy (HSQC and HMQC) / Jonathan A. Iggo ; Jianke Liu ; Gillian Overend |
| 2D NMR Spectroscopy |
| Spin Systems |
| Review of Recent Reports of the Indirect Detection of Metal Nuclei |
| Theoretical and Experimental Studies on 19F NMR Shieldings in Mineral Glasses, Zeolites and Related Silsequioxanes / J.A. TossellChapter 1： |
| NOE Studies of Solvent-Solute Interactions / J.T. GerigChapter 2： |
| DFT Computations of Transition Metal Chemical Shifts / Michael Buehl ; Muelheim an der RuhrChapter 3： |
| Solid-State NMR Studies of Collagen Structure and Dynamics in Isolated Fibrils and in Biological Tissues / Daniel Huster ; Halle-WittembergChapter 4： |
| NMR Studies of Beverage / J. Kidric ; LjubljanaChapter 5： |
| Contribution of NMR Spectroscopy to Flavour Release and Perception / L. Tavel ; E. Guichard ; C. Moreau ; DijonChapter 6： |
| Polymer Blend Miscibility / Jeffrey L. WhiteChapter 7： |
| Quantitative 2D NMR Studies / Harri Koskela |
| Concepts |
| Recent Advances in Solvent Suppression for Solution NMR: A Practical Reference / Ryan T. Mckay |
| Rationale |
| Solvent Suppression |
| Suppression Pulse Sequences |
| Comparisons, Conclusions, and Advice |
| Photo-CIDNP Spectroscopy / Martin Goez |
| CIDNP Phenomena |
| CIDNP Theory |
| Instrumentation and Techniques |
| Chemical Information Obtainable by High-Field CIDNP |
| Recent Applications of CIDNP to Chemical and Biochemical Problems |
| Techniques Used for 14N NQR Studies / V. Mikhaltsevitch |
| Short-repetition Time Sequences in NQR of Nitrogen |
| Polarization Enhancement of NQR Signals |
| Multi-pulse Sequences Under Conditions of Magneto-acoustic and Piezo-Electric Ringing |
| Chlorine, Bromine, and Iodine Solid-State NMR Spectroscopy / Cory M. Widdifield ; Rebecca P. Chapman ; David L. Bryce |
| Theoretical Background |
| Experimental and Computational Methods |
| Survey of Available Experimental Data |
| Relativistic Computations of NMR Parameters from First Principles. Theory and Applications' / J.Autschbach ; S.Zheng |
| Applications of Silicon-Carbon Coupling Constants / V.Blechta |
| One Dimensional Double Quantum Filter NMR Studies / N.Chandrakumar |
| Analysis of Proton NMR Spectra of Strongly and Weakly Dipolar Coupled Spins: Special Emphasis on Spectral Simplification, Chiral Discrimination and Discerning of Degenerate Transitions / B.BaisHya(1) ; U.R.Prabhu (1,2) ; N.Suryaprakash (1) |
| Applications of 33S NMR Spectroscopy / Roberta Musio |
| NMR Spectroscopic Properties of Sulphur-33 |
| 33S NMR Parameters |
| 33S NMR Parameters and Molecular Structure |
| Theoretical Calculations of 33S NMR Parameters |
| Appendix |
| NMR of Peptide Toxins / K. Johan Rosengren ; Norelle L. Daly ; David J. Craik |
| NMR as a Tool for Determining the Structures of Toxins |
| Microbial Toxins |
| Plant Toxins |
| Animal Toxins |
| Conclusions and Outlook |
| Application of NMR Spectroscopy in Isotope Effects Studies / Stefan Jankowski |
| Isotope Effects on Chemical Shifts and Spin-Spin Coupling Constants |
| Kinetic Isotope Effects Measured at Natural Abundance |
| Kinetic Isotope Effect Studies of Reaction Mechanisms by NMR Spectroscopy |
| Residual Dipolar Couplings for the Configurational and Conformational Analysis of Organic Molecules / G. Kummerlöwe ; B. Luy |
| Alignment Media for Weak Alignment |
| Scaling of Alignment |
| Pulse Sequences |
| Conclusion and Outlook |
| See Color Plate Section at the end of this book |
| Recent Developments in Liquid-State Inadequate Studies / Dušan Uhrír |
| Inadequate-The Basic Concept |
| Increasing the Sensitivity of Inadequate |
| Measurement of 13C-13C Coupling Constants |
| Applications of High-Resolution Inadequate to 13C |
| Applications of Inadequate to Nuclei Other Than 13C |
| Outlook |
| Phosphorus-31 NMR Spectroscopy of Condensed Matter / Marek J. Potrzebowski ; Slawomir Kazmierski ; Hassan Kassassir ; Beata Miksa |
| Progress in Methodology |
| Applications of 31P SS NMR Spectroscopy |
| Recent Applications of Solid-State 17O NMR / K. Yamada |
| 17O Synthesis |
| Background of solid-State 17O NMR |
| Fundamentals of 17O NMR in Biological Solids |
| Applications of Solid-State 17O NMR in Biochemistry |
| Spatial Inhomogeneity of Cavities in Polymer Network Systems as Characterised by Field-Gradient NMR Using Probe Diffusant Molecules and Polymers with Different Sizes / Kazuhiro Kamiguchi ; Shigeki Kuroki ; Yuji Yamane ; Mitsuru Satoh ; Isao Ando |
| Network Structure of Polymer Gets and Diffusional Behaviour of probe polymers |
| Network Structure of Micrometre-Scale Cavity Obtained from Phase-Separated Polymer Blends as Characterised by Using Probe Molecules |
| Practical NMR Analysis of Morphology and Structure of Polymers / Takeshi Yamanobe ; Hiroki Uehara ; Masaki Kakiage |
| Analysis Method of Free Induction Decay of 1H Pulse NMR for Polymers |
| Morphology and Relaxation Behaviour |
| Kinetics of Dynamic Process of Polymers |
| Microporous Carbon Materials / K. V. Romanenko |
| Mesoporous Carbon Materials |
| NMR Studies for Mapping Structure and Dynamics of Nucleosides in Water / Bernard Ancian |
| Nomenclature and Symbols |
| About Stacking of Nucleosides in Water |
| Structure in Water |
| Dynamics in Water |
| Time-Domain NMR Applied to Food Products / J. van Duynhoven ; A. Voda ; M. Witek ; H. Van As |
| History |
| Equipment |
| One-Dimensional Relaxometry and Diffusometry |
| Two-Dimensional NMR Diffusometry and Relaxometry |
| Data-Analysis Approaches |
| Benchtop Time-Domain NMR Applications |
| Mobile Time-Domain NMR Applications |
| Perspectives and Conclusions |
| From Helical Jump to Chain Diffusion: Solid-State NMR Study of Chain Dynamics in Semi-Crystalline Polymers / Yefeng Yao |
| NMR Strategies for Probing Chain Dynamics in Solid Polymeric Materials |
| Helical Jump and Chain Diffusion in Semi-Crystalline Polymers |
| Recent Developments in HMBC (Heteronuclear Multiple Bond Correlation) Experiments / Norbert Müller ; Wolfgang Schoefberger ; Judith Schlagnitweit |
| Two Dimensional Higher Quantum Correlation and Resolved Techniques for the Analyses of Complex 1H NMR Spectra of Scalar Coupled Spins / N. Suryaprakash |
| High Resolution Magic Angle Spinning | Enabling Applications of NMR Spectroscopy to Semi-Solid Phases / William P. Power |
| Accurate measurement of small J couplings / Zhong Chen ; Yuqing Huang ; Yanqin Lin ; Shuhui Cai |
| High-resolution 1H NMR spectroscopy of solids / Paul Hodgkinson |
| Multiple-Wave-Vector Diffusion-Weighted NMR / J¿urgen Finsterbusch |
| Constant Time REDOR NMR Spectroscopy / Thomas Echelmeyer ; Sebastian Wegner ; Leo van Wüllen |
| Recent advances in solid-state 25Mg NMR spectroscopy / Jair C. C. Freitas ; Mark E. Smith |
| Methods and Applications of Phosphorus NMR Spectroscopy in Vivo / Jing-Huei Lee ; Richard A. Komoroski ; Wen-Jang Chu ; Jonathan A. Dudley |
| Compact superconducting magnet design for nuclear magnetic resonance: The minimum stored energy (MSE) approach / Quang M. Tieng ; Viktor Vegh |
| Getting the Most Out of HSQC and HMBC Spectra / William F. Reynolds ; Darcy C. Burns |
| A Review of REDCRAFT: Simultaneous Investigation of Structure and Dynamics of Proteins from RDC Restraints / Homayoun Valafar ; Mikhail Simin ; Stephanie Irausquin |
| NMR Studies of Solid State Dynamics / Danuta Kruk ; Alexei Privalov ; Wojciech Medycki ; Cezary Uniszkiewicz ; Wlodzimierz Masierak ; Ryszard Jakubas |
| Earth's Field Spectroscopy / Mark Hunter |
| Recent Advances in Nuclear Shielding Calculations / Angel C. de Dios ; Cynthia J. Jameson |
| Pure Phase Encode Magnetic Resonance Imaging of Fluids in Porous Media / Colleen E. Muir ; Bruce J. Balcom |
| Steroids and NMR / Martin Jaeger ; Ruud L.E.G. Aspers |
| Structural Characterization of Zeolites by Advanced Methods of Solid State NMR Spectroscopy / Luís Mafra ; José Alejandro Vidal-Moya ; Teresa Blasco |
| Recent Progress in the Solid-State NMR Studies of Biomineralization / Tim W. T. Tsai ; Jerry C. C. Chan |
| Recent advances in the NMR spectroscopy of chlorine, bromine and iodine / Bradley J. Butler ; James M. Hook ; Jason B. Harper |
| Solution-State Dynamic Nuclear Polarization / Mark D. Lingwood ; Songi Han |
| Solid-state NMR of membrane proteins: moving towards greater complexity / Lynmarie K. Thompson |
| Chromatographic NMR / Stefano Caldarelli |
| Kinetic Monte Carlo Simulation of DNMR Spectra / Zsófia Szalay ; János Rohonczy |
| NMR Studies of Antimicrobial Peptides / H.J. Vogel ; E.F. Haney |
| NMR Studies of Protein Folding Prof / M. Demura* ; M. Miguguchi ; K. Kauvans |
| Applications of NOE in Molecular Biology Prof / M.P. Williamson |
| Recent Applications of REDOR to Biological Problems Prof / T. Gullion |
| Electrophoretic NMR-Ions, Molecules, Mixtures, Pores and Complexes / P. C. Griffiths |
| Two Dimensional NMR on Biopsy and In Vivo / S. Ramadan ; C.E. Mountford |
