High resolution NMR : theory and chemical applications

>> Google Books

所蔵情報QRコード

High resolution NMR : theory and chemical applications / Edwin D. Becker

版:: 3rd ed
資料種別:: 図書
出版情報:: San Diego : Academic Press, c2000
形態:: xvi, 424 p. ; 24 cm
著者名:: Becker, Edwin D. <DA00663460>
ISBN:: 9780120846627 [0120846624]
書誌ID:: BA44106567

子書誌情報

フルテキスト

所蔵情報

他の版・巻

High resolution NMR : theory and chemical applications. 2nd ed (: pbk)
Edwin D. Becker , Academic Press , 1980

High resolution NMR : theory and chemical applications
[by] Edwin D. Becker , Academic Press , [1969]

書誌詳細

注記:

Includes bibliographical references and index

主題:

Nuclear magnetic resonance spectroscopy

言語:

英語

目次情報:

Preface to the Third Edition

Introduction / 1：

Origins and Early History of NMR / 1.1：

High Resolution NMR: An Overview / 1.2：

Additional Reading and Resources / 1.3：

The Theory of NMR / 2：

Nuclear Spin and Magnetic Moment / 2.1：

Theoretical Descriptions of NMR / 2.2：

Steady-State Quantum Mechanical Description / 2.3：

Effect of the Boltzmann Distribution / 2.4：

Spin-Lattice Relaxation / 2.5：

Precession of Nuclear Magnetic Moments / 2.6：

Classical Mechanical Description of NMR / 2.7：

Magnetization in the Rotating Frame / 2.8：

Methods of Obtaining NMR Spectra / 2.9：

Dynamic Processes / 2.10：

Terminology, Symbols, Units, and Conventions / 2.11：

Problems / 2.12：

Instrumentation and Techniques / 3：

Advantages of Pulse Fourier Transform NMR / 3.1：

Basic NMR Apparatus / 3.2：

Requirements for High Resolution NMR / 3.3：

Detection of NMR Signals / 3.4：

Phase Cycling / 3.5：

Fourier Transformation of the FID / 3.6：

Data Acquisition / 3.7：

Data Processing / 3.8：

Digital Filtering / 3.9：

Alternatives to Fourier Transformation / 3.10：

Sensitivity and Size of Sample / 3.11：

Useful Solvents / 3.12：

Chemical Shifts / 3.13：

The Origin of Chemical Shifts / 4.1：

Theory of Chemical Shifts / 4.2：

Measurement of Chemical Shifts / 4.3：

Empirical Correlations of Chemical Shifts / 4.4：

Some Aspects of Proton Chemical Shifts / 4.5：

Nuclei Other Than Hydrogen / 4.6：

Compilations of Spectral Data and Empirical Estimates of Chemical Shifts / 4.7：

Isotope Effects / 4.8：

Effects of Molecular Asymmetry / 4.9：

Paramagnetic Species / 4.10：

Coupling between Pairs of Spins / 4.11：

Origin of Spin Coupling Interactions / 5.1：

General Aspects of Spin-Spin Coupling / 5.2：

Theory of Spin-Spin Coupling / 5.3：

Correlation of Coupling Constants with Other Physical Properties / 5.4：

Effect of Exchange / 5.5：

Spin Decoupling and Double Resonance / 5.6：

Structure and Analysis of Complex Spectra / 5.7：

Symmetry and Equivalence / 6.1：

Notation / 6.2：

Energy Levels and Transitions in an AX System / 6.3：

Quantum Mechanical Treatment / 6.4：

The Two-Spin System without Coupling / 6.5：

Factoring the Secular Equation / 6.6：

Two Coupled Spins / 6.7：

The AB Spectrum / 6.8：

AX, AB, and A[subscript 2] Spectra / 6.9：

"First-Order" Spectra / 6.10：

Symmetry of Spin Wave Functions / 6.11：

General Procedures for Simulating Spectra / 6.12：

Three-Spin Systems / 6.13：

Relative Signs of Coupling Constants / 6.14：

Some Consequences of Strong Coupling and Chemical Equivalence / 6.15：

"Satellites" from Carbon-13 and Other Nuclides / 6.16：

The AA'BB' and AA'XX' Systems / 6.17：

Spectra of Solids / 6.18：

Spin Interactions in Solids / 7.1：

Dipolar Interactions / 7.2：

"Scalar Coupling" / 7.3：

The Heteronuclear Two-Spin System / 7.4：

Dipolar Decoupling / 7.5：

Cross Polarization / 7.6：

The Homonuclear Two-Spin System / 7.7：

Line Narrowing by Multiple Pulse Methods / 7.8：

Anisotropy of the Chemical Shielding / 7.9：

Magic Angle Spinning / 7.10：

Quadrupole Interactions and Line-Narrowing Methods / 7.11：

Other Aspects of Line Shapes / 7.12：

Orientation Effects in Liquids: Liquid Crystals / 7.13：

Relaxation / 7.14：

Molecular Motions and Processes for Relaxation in Liquids / 8.1：

Nuclear Magnetic Dipole Interactions / 8.2：

Nuclear Overhauser Effect / 8.3：

Relaxation via Chemical Shielding Anisotropy / 8.4：

Electric Quadrupole Relaxation / 8.5：

Scalar Relaxation / 8.6：

Spin-Rotation Relaxation / 8.7：

Relaxation by Paramagnetic Substances / 8.8：

Other Factors Affecting Relaxation / 8.9：

Pulse Sequences / 8.10：

The Spin Echo / 9.1：

The Carr-Purcell Pulse Sequence / 9.2：

Correcting for Pulse Imperfections / 9.3：

Spin Locking / 9.4：

Selective Excitation / 9.5：

Decoupling / 9.6：

Polarization Transfer Methods / 9.7：

Two-Dimensional NMR / 9.8：

General Aspects of 2D Spectra / 10.1：

A Survey of Basic 2D Experiments / 10.2：

Data Acquisition and Processing / 10.3：

Sensitivity Considerations / 10.4：

Density Matrix and Product Operator Formalisms / 10.5：

The Density Matrix / 11.1：

Transformations of the Density Matrix / 11.2：

The One-Spin System / 11.3：

The Two-Spin System / 11.4：

INEPT and Related Pulse Sequences / 11.5：

Product Operators / 11.6：

Coherence Transfer Pathways / 11.7：

Selected 1D, 2D, and 3D Experiments: A Further Look / 11.8：

Spectral Editing / 12.1：

Double Quantum Filtering Experiments / 12.2：

COSY / 12.3：

Heteronuclear Correlation by Indirect Detection / 12.4：

Three- and Four-Dimensional NMR / 12.5：

Elucidation of Molecular Structure and Macromolecular Conformation / 12.6：

Organic Structure Elucidation / 13.1：

Application of Some Useful 2D Methods / 13.2：

Structure and Configuration of Polymers / 13.3：

Three-Dimensional Structure of Biopolymers / 13.4：

NMR Imaging and Spatially Localized Spectroscopy / 13.5：

Use of Magnetic Field Gradients to Produce Images / 14.1：

Use of 2D NMR Methods in Imaging / 14.2：

k Space; Echo Planar Imaging / 14.3：

Factors Affecting Image Contrast / 14.4：

Chemical Shift Imaging and in Vivo Spectroscopy / 14.5：

NMR Imaging in Solids / 14.6：

Properties of Common Nuclear Spins / 14.7：

ABX and AA'XX' Spectra / Appendix B：

The ABX System / B.1：

The AA'XX' System / B.2：

Review of Relevant Mathematics / Appendix C：

Complex Numbers / C.1：

Trigonometric Identities / C.2：

Vectors / C.3：

Matrices / C.4：

Spin Matrices / Appendix D：

One Spin / D.1：

Two-Spin System / D.2：

Selected Answers to Problems / Appendix E：

References

Index

Preface to the Third Edition

Introduction / 1：

Origins and Early History of NMR / 1.1：

High Resolution NMR: An Overview / 1.2：

Additional Reading and Resources / 1.3：

The Theory of NMR / 2：

続きを見る

ブックレビュー

類似資料:

1 図書 High resolution NMR : theory and chemical applications (: pbk) Becker, Edwin D. Academic Press	7 図書 High-resolution solid-state NMR of silicates and zeolites Engelhardt, Günter, Michel, Dieter J. Wiley
2 図書 High resolution NMR : theory and chemical applications Becker, Edwin D. Academic Press	8 図書 Modern techniques in high resolution FT-NMR Chandrakumar, N., 1951-, Subramanian, S., 1942- Springer-Verlag
3 図書 High-resolution NMR techniques in organic chemistry (: pbk ; : hbk) Claridge, Timothy D. W. Elsevier	9 図書 High resolution NMR spectroscopy of synthetic polymers in bulk (: VCH Publishers ; : VCH Verlagsgesellschaft) Komoroski, Richard A., 1947- VCH Publishers
4 図書 The analysis of high resolution NMR spectra Abraham, Raymond J. Elsevier Pub. Co.	10 図書 High resolution NMR in solids : selective averaging Ulrich, Haeberlen Academic Press
5 図書 High resolution NMR spectroscopy in solids (: us ; : gw) Mehring, M., 1937-, Diehl, Peter, Fluck, Ekkehard, Kosfeld, R. Springer-Verlag	11 図書 Quantum description of high-resolution NMR in liquids (: hbk ; : pbk) Goldman, M. (Maurice), 1933- Clarendon Press, Oxford University Press
6 図書 Principles of high resolution NMR in solids (: us ; : gw ; : pbk) Mehring, M., 1937- Springer-Verlag	12 電子ブック NMR spectroscopy explained : simplified theory, applications and examples for organic chemistry and structural biology Jacobsen, Neil E. Wiley Online Library