Sample preparation in chromatography

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Sample preparation in chromatography / Serban C. Moldoveanu, Victor David

資料種別:

図書

出版情報:

Amsterdam ; Tokyo : Elsevier, 2002

形態:

xi, 930 p. ; 25cm

シリーズ名:

Journal of chromatography library ; v. 65 <BA00154245>

著者名:

ISBN:

9780444503947 [0444503943]

書誌ID:

BA58057459

子書誌情報

フルテキスト

所蔵情報

他の版・巻

書誌詳細

注記:

Includes index

言語:

英語

目次情報:

Introduction and General Considerations / Part 1.：

Preparatory Information / 1.：

Overview of a Chemical Analysis / 1.1.：

Types of Operations Used in Sample Preparation / 1.2.：

Some Theoretical Aspects of Phase Transfers / 1.3.：

Introductory Approach to Theory of Distribution Equilibria / 1.4.：

Some Aspects of Mass Transfer Processes / 1.5.：

Characterization of Chromatographic Separations / 1.6.：

General Characteristics of Separations / 1.7.：

Elementary Discussion on Thermodynamic and Kinetic Factors in Chemical Reactions / 1.8.：

Brief Survey on Molecular Interactions / 1.9.：

Empirical and Estimated Parameters for Sample Preparation Problems / 1.10.：

Introductory Discussion on Precision, Accuracy, Sensitivity, and Limit of Detection in Chemical Analysis / 1.11.：

Validation of an Analytical Method / 1.12.：

References 1

Sampling and Its Connection with Sample Preparation / 2.：

Relation of Sampling to Sample Preparation / 2.1.：

Representative Samples / 2.2.：

Techniques for Sample Collection / 2.3.：

Handling, Preservation, and Storage of Samples / 2.4.：

References 2

Overview on Sample Preparation for Chromatography / 3.：

The Role of Sample Preparation / 3.1.：

The Use of Preliminary Information for the Choice of a Sample Preparation Procedure / 3.2.：

Sample Homogenization and Dissolution / 3.3.：

Sample Cleanup, Fractionation, and Concentration / 3.4.：

Chemical Modifications of the Sample / 3.5.：

Other Types of Sample Modifications / 3.6.：

Differences in Sample Preparation for Different Chromatographic Techniques / 3.7.：

Quantitation Techniques in Chromatography and Their Relation to Sample Preparation / 3.8.：

Method Development in Sample Preparation / 3.9.：

References 3

Chromatography as the Core Step in an Analytical Process / 4.：

The Choice of the Core Analytical Technique / 4.1.：

Gas Chromatography as a Core Step in the Analytical Process / 4.2.：

Conventional High Performance Liquid Chromatography as a Core Analytical Technique / 4.3.：

Other Chromatography Types Used as a Core Analytical Technique / 4.4.：

References 4

Data Processing in Chromatographic Methods / 5.：

Information Gain from Chromatographic Data / 5.1.：

Qualitative and Quantitative Data from the Chromatographic Process / 5.2.：

References 5

Automation in Sample Preparation / 6.：

Automation in the Instrumentation Used in Sample Preparation / 6.1.：

Computer Assisted Method Development / 6.2.：

References 6

Sample Preparation Techniques Using Physical Processes / Part 2.：

Mechanical Processing in Sample Preparation / 7.：

Grinding, Sieving, and Blending / 7.1.：

Filtration, Microfiltration, and Ultrafiltration / 7.2.：

Centrifugation / 7.3.：

References 7

Phase Transfer Separations Applied in Sample Preparations / 8.：

Distillation, Vaporization, and Drying / 8.1.：

Dissolution, Crystallization, and Precipitation / 8.2.：

References 8

Headspace Sampling Techniques in Gas Chromatography / 9.：

Static Headspace Techniques / 9.1.：

Dynamic Headspace / 9.2.：

Other Headspace Techniques / 9.3.：

References 9

Solvent Extraction / 10.：

Liquid-Liquid Extraction / 10.1.：

Conventional Liquid-Solid Extraction / 10.2.：

Accelerated Solvent Extraction / 10.3.：

Microwave-Assisted Solvent Extraction / 10.4.：

Simultaneous Distillation and Extraction / 10.5.：

Supercritical Solvent Extraction / 10.6.：

References 10

Sorbent Extraction / 11.：

Solid Phase Extraction Procedures / 11.1.：

Solid Phase Microextraction / 11.2.：

Matrix Solid Phase Dispersion / 11.3.：

Other Solid Phase Sample Preparation Techniques / 11.4.：

References 11

Chromatographic Procedures as Preliminary Separation / 12.：

Gas Chromatography as a Sample Preparation Technique and Bidimensional GC / 12.1.：

Liquid Chromatography as a Sample Preparation Technique / 12.2.：

Size Exclusion Used in Sample Preparation / 12.3.：

References 12

Membrane Separations / 13.：

Gas Diffusion through Membranes and Stripping / 13.1.：

Reverse Osmosis and Dialysis / 13.2.：

References 13

Electroseparation Techniques in Sample Preparation / 14.：

Electrophoretic Techniques / 14.1.：

Other Electroseparation Techniques / 14.2.：

References 14

Other Separation Techniques in Sample Preparation / 15.：

Ion Exchange in Sample Preparation / 15.1.：

Other Techniques in Sample Preparation / 15.2.：

References 15

Sample Preparation Techniques Involving Chemical Modifications / Part 3.：

Chemical Modifications for Dissolution and Fractionation / 16.：

Chemical Modifications for Sample Dissolution / 16.1.：

Changes in pH and Chemical Modifications for Fractionation Purposes / 16.2.：

References 16

Purpose of Derivatization in Chromatographic Analysis / 17.：

General Aspects Regarding Derivatization / 17.1.：

Preparation of the Sample for Derivatization and Common Derivatization Labware / 17.2.：

Derivatization for Improving Gas Chromatographic Process / 17.3.：

Derivatization for Improving Detection in GC / 17.4.：

Derivatization for Improving Mass Spectral Identification / 17.5.：

Derivatization for Improving Detection in HPLC and TLC / 17.6.：

Derivatization for Chiral Separations / 17.7.：

References 17

Chemical Reactions Used in Derivatization / 18.：

Reactions with Formation of Alkyl or Aryl Derivatives / 18.1.：

Silylation Reactions / 18.2.：

Acylation Reactions / 18.3.：

Reactions of Addition to Carbon-Heteroatom Multiple Bonds Used for Derivatization / 18.4.：

Derivatization Reactions with Formation of Cyclic Compounds / 18.5.：

Other Derivatization Reactions / 18.6.：

Derivatization Reactions Involving Solid Phase Reagents / 18.7.：

Derivatization on a Solid Support / 18.8.：

References 18

Derivatization Reactions for Analytes with Various Functional Groups / 19.：

Derivatization of Compounds with Alcohols, Epoxide, or Ether Groups / 19.1.：

Derivatization Reactions for Phenols / 19.2.：

Derivatization Reactions for Thiols and Sulfides / 19.3.：

Derivatization of Compounds with Amino and Other Nitrogen-Containing Groups / 19.4.：

Derivatization of Aldehydes and Ketones / 19.5.：

Derivatization of Carboxylic Acids / 19.6.：

Derivatization of Amides, Esters, and Other Derivatives of Carboxylic Acids, and of Carbonic Acid / 19.7.：

Derivatization of Other Types of Organic Groups and of Organometallic and Inorganic Compounds / 19.8.：

Derivatization of Carbohydrates / 19.9.：

Derivatization of Amino Acids and Related Compounds / 19.10.：

Derivatization of Other Multifunctional Compounds / 19.11.：

References 19

Chemical Degradation of Polymers and Pyrolysis / 20.：

Chemical Degradation of Polymeric Carbohydrates / 20.1.：

Chemical Degradation of Proteins for Analytical Purposes / 20.2.：

Chemical Degradation of other Macromolecular Compounds / 20.3.：

Overview of Analytical Pyrolysis / 20.4.：

Pyrolysis as a Chemical Modification Technique / 20.5.：

Instrumentation Used in Analytical Pyrolysis / 20.6.：

Application of Analytical Pyrolysis / 20.7.：

References 20

Symbols, Units, and Constants

Index

Introduction and General Considerations / Part 1.：

Preparatory Information / 1.：

Overview of a Chemical Analysis / 1.1.：

Types of Operations Used in Sample Preparation / 1.2.：

Some Theoretical Aspects of Phase Transfers / 1.3.：

Introductory Approach to Theory of Distribution Equilibria / 1.4.：

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