Introduction / 1: |
Fundamentals / 2: |
Sample Preparation / 2.1: |
Solid Phase Extraction / 2.1.1: |
Solid Phase Microextraction / 2.1.1.1: |
Supercritical Fluid Extraction / 2.1.2: |
Pressurized Fluid Extraction / 2.1.3: |
Online Liquid Chromatography Clean-up / 2.1.4: |
Headspace Techniques / 2.1.5: |
Static Headspace Technique / 2.1.5.1: |
Dynamic Headspace Technique (Purge and Trap) / 2.1.5.2: |
Headspace versus Purge and Trap / 2.1.5.3: |
Adsorptive Enrichment and Thermodesorption / 2.1.6: |
Sample Collection / 2.1.6.1: |
Calibration / 2.1.6.2: |
Desorption / 2.1.6.3: |
Pyrolysis and Thermal Extraction / 2.1.7: |
Foil Pyrolysis / 2.1.7.1: |
Curie Point Pyrolysis / 2.1.7.2: |
Thermal Extraction / 2.1.7.3: |
Gas Chromatography / 2.2: |
Fast Gas Chromatography / 2.2.1: |
Fast Chromatography / 2.2.1.1: |
Ultra Fast Chromatography / 2.2.1.2: |
Two Dimensional Gas Chromatography / 2.2.2: |
Heart Cutting / 2.2.2.1: |
Comprehensive GC x GC / 2.2.2.2: |
Modulation / 2.2.2.3: |
Detection / 2.2.2.4: |
Data Handling / 2.2.2.5: |
Moving Capillary Stream Switching / 2.2.2.6: |
GC/MS Sample Inlet Systems / 2.2.3: |
Carrier Gas Regulation / 2.2.3.1: |
The Microseal Septum / 2.2.3.2: |
Hot Sample Injection / 2.2.3.3: |
Cold Injection Systems / 2.2.3.4: |
Injection Volumes / 2.2.3.5: |
On-column Injection / 2.2.3.6: |
Cryofocusing / 2.2.3.7: |
Capillary Columns / 2.2.4: |
Sample Capacity / 2.2.4.1: |
Internal Diameter / 2.2.4.2: |
Film Thickness / 2.2.4.3: |
Column Length / 2.2.4.4: |
Adjusting the Carrier Gas Flow / 2.2.4.5: |
Properties of Stationary Phases / 2.2.4.6: |
Chromatography Parameters / 2.2.5: |
The Chromatogram and its Meaning / 2.2.5.1: |
Capacity Factor k' / 2.2.5.2: |
Chromatographic Resolution / 2.2.5.3: |
Factors Affecting the Resolution / 2.2.5.4: |
Maximum Sample Capacity / 2.2.5.5: |
Peak Symmetry / 2.2.5.6: |
Optimisation of Flow / 2.2.5.7: |
Classical Detectors for GC/MS Systems / 2.2.6: |
FID / 2.2.6.1: |
NPD / 2.2.6.2: |
ECD / 2.2.6.3: |
PID / 2.2.6.4: |
ELCD / 2.2.6.5: |
FPD / 2.2.6.6: |
PDD / 2.2.6.7: |
Connection of Classical Detectors Parallel to the Mass Spectrometer / 2.2.6.8: |
Mass Spectrometry / 2.3: |
Resolving Power and Resolution in Mass Spectrometry / 2.3.1: |
High Resolution / 2.3.1.1: |
Unit Mass Resolution / 2.3.1.2: |
High and Low Resolution in the Case of Dioxin Analysis / 2.3.1.3: |
Time-of-Flight Analyser / 2.3.2: |
Isotope Ratio Monitoring GC/MS / 2.3.3: |
Ionisation Procedures / 2.3.4: |
Electron Impact Ionisation / 2.3.4.1: |
Chemical Ionisation / 2.3.4.2: |
Measuring Techniques in GC/MS / 2.3.5: |
Detection of the Complete Spectrum (Full Scan) / 2.3.5.1: |
Recording Individual Masses (SIM/MID) / 2.3.5.2: |
High Resolution Accurate Mass MID Data Acquisition / 2.3.5.3: |
MS/MS - Tandem Mass Spectrometry / 2.3.6: |
Mass Calibration / 2.3.7: |
Special Aspects of GC/MS Coupling / 2.4: |
Vacuum Systems / 2.4.1: |
GC/MS Interface Solutions / 2.4.2: |
Open Split Coupling / 2.4.2.1: |
Direct Coupling / 2.4.2.2: |
Separator Techniques / 2.4.2.3: |
References for Chapter 2 |
Evaluation of GC/MS Analyses / 3: |
Display of Chromatograms / 3.1: |
Total Ion Current Chromatograms / 3.1.1: |
Mass Chromatograms / 3.1.2: |
Substance Identification / 3.2: |
Extraction of Mass Spectra / 3.2.1: |
The Retention Index / 3.2.2: |
Libraries of Mass Spectra / 3.2.3: |
Universal Mass Spectral Libraries / 3.2.3.1: |
Application Libraries of Mass Spectra / 3.2.3.2: |
Library Search Procedures / 3.2.4: |
The INCOS/NIST Search Procedure / 3.2.4.1: |
The PBM Search Procedure / 3.2.4.2: |
The SISCOM Procedure / 3.2.4.3: |
Interpretation of Mass Spectra / 3.2.5: |
Isotope Patterns / 3.2.5.1: |
Fragmentation and Rearrangement Reactions / 3.2.5.2: |
DMOX Derivatives for Location of Double Bond Positions / 3.2.5.3: |
Mass Spectroscopic Features of Selected Substance Classes / 3.2.6: |
Volatile Halogenated Hydrocarbons / 3.2.6.1: |
Benzene/Toluene/Ethylbenzene/Xylenes (BTEX, Alkylaromatics) / 3.2.6.2: |
Polyaromatic Hydrocarbons (PAH) / 3.2.6.3: |
Phenols / 3.2.6.4: |
Pesticides / 3.2.6.5: |
Polychlorinated Biphenyls (PCBs) / 3.2.6.6: |
Polychlorinated Dioxins/Furans (PCDDs/PCDFs) / 3.2.6.7: |
Drugs / 3.2.6.8: |
Explosives / 3.2.6.9: |
Chemical Warfare Agents / 3.2.6.10: |
Brominated Flame Retardants (BFR) / 3.2.6.11: |
Quantitation / 3.3: |
Decision Limit / 3.3.1: |
Limit of Detection / 3.3.2: |
Limit of Quantitation / 3.3.3: |
Sensitivity / 3.3.4: |
The Calibration Function / 3.3.5: |
Quantitation and Standardisation / 3.3.6: |
External Standardization / 3.3.6.1: |
Internal Standardisation / 3.3.6.2: |
The Standard Addition Procedure / 3.3.6.3: |
Frequently Occurring Impurities / 3.4: |
References for Chapter 3 |
Applications / 4: |
Air Analysis According to EPA Method TO-14 / 4.1: |
BTEX Using Headspace GC/MS / 4.2: |
Simultaneous Determination of Volatile Halogenated Hydrocarbons and BTEX / 4.3: |
Static Headspace Analysis of Volatile Priority Pollutants / 4.4: |
MAGIC 60 - Analysis of Volatile Organic Compounds / 4.5: |
irm-GC/MS of Volatile Organic Compounds Using Purge and Trap Extraction / 4.6: |
Vinyl Chloride in Drinking Water / 4.7: |
Chloral Hydrate in Surface Water / 4.8: |
Field Analysis of Soil Air / 4.9: |
Residual Monomers and Polymerisation Additives / 4.10: |
Geosmin and Methylisoborneol in Drinking Water / 4.11: |
Substituted Phenols in Drinking Water / 4.12: |
GC/MS/MS Target Compound Analysis of Pesticide Residues in Difficult Matrices / 4.13: |
Multi-component Pesticide Analysis by MS/MS / 4.14: |
Multi-method for the Determination of 239 Pesticides / 4.15: |
Nitrophenol Herbicides in Water / 4.16: |
Dinitrophenol Herbicides in Water / 4.17: |
Hydroxybenzonitrile Herbicides in Drinking Water / 4.18: |
Routine Analysis of 24 PAHs in Water and Soil / 4.19: |
Fast GC Quantification of 16 EC Priority PAH Components / 4.20: |
Analysis of Water Contaminants by On-line SPE-GC/MS / 4.21: |
Determination of Polar Aromatic Amines by SPME / 4.22: |
Congener Specific Isotope Analysis of Technical PCB Mixtures / 4.23: |
Polychlorinated Biphenyls in Indoor Air / 4.24: |
Confirmation Analysis of Dioxins and Dioxin-like PCBs / 4.25: |
Fast GC Analysis for PCBs / 4.26: |
Analysis of Brominated Flame Retardants PBDE / 4.27: |
Trace Analysis of BFRs in Waste Water Using SPME-GC/MS/MS / 4.28: |
Analysis of Military Waste / 4.29: |
Detection of Drugs in Hair / 4.30: |
Detection of Morphine Derivatives / 4.31: |
Detection of Cannabis Consumption / 4.32: |
Analysis of Steroid Hormones Using MS/MS / 4.33: |
Determination of Prostaglandins Using MS/MS / 4.34: |
Detection of Clenbuterol by CI / 4.35: |
General Unknown Toxicological-chemical Analysis / 4.36: |
Clofibric Acid in Aquatic Systems / 4.37: |
Polycyclic Musks in Waste Water / 4.38: |
Identification and Quantification of Trichothecene Mycotoxins / 4.39: |
Highly Sensitive Screening and Quantification of Environmental Components Using Chemical Ionisation with Water / 4.40: |
Characterization of Natural Waxes by Pyrolysis-GC/MS / 4.41: |
Quantitative Determination of Acrylate Copolymer Layers / 4.42: |
References for Chapter 4 |
Glossary / 5: |
Subject Index |
Introduction / 1: |
Fundamentals / 2: |
Sample Preparation / 2.1: |