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1.

電子ブック

EB
Neil E Jacobsen
出版情報: Wiley Online Library  1 online resource (xv, 668 p.)
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Preface
Acknowledgments
Fundamentalsof NMR Spectroscopy in Liquids / 1:
Introduction to NMR Spectroscopy / 1.1:
Examples: NMR Spectroscopy of Oligosaccharides and Terpenoids / 1.2:
Typical Values of Chemical Shifts and Coupling Constants / 1.3:
Fundamental Concepts of NMR Spectroscopy / 1.4:
Interpretation of Proton (1H) NMR Spectra / 2:
Assignment / 2.1:
Effect of Bo Field Strength on the Spectrum / 2.2:
First-Order Splitting Patterns / 2.3:
The Use of 1H-1H Coupling Constants to Determine Stereochemistry and Conformation / 2.4:
Symmetry and Chirality in NMR / 2.5:
The Origin of the Chemical Shift / 2.6:
J Coupling to Other NMR-Active Nuclei / 2.7:
Non-First-Order Splitting Patterns: Strong Coupling / 2.8:
Magnetic Equivalence / 2.9:
NMR Hardware and Software / 3:
Sample Preparation / 3.1:
Sample Insertion / 3.2:
The Deuterium Lock Feedback Loop / 3.3:
The Shim System / 3.4:
Tuning and Matching the Probe / 3.5:
NMR Data Acquisition and Acquisition Parameters / 3.6:
Noise and Dynamic Range / 3.7:
Special Topic: Oversampling and Digital Filtering / 3.8:
NMR Data Processing-Overview / 3.9:
The Fourier Transform / 3.10:
Data Manipulation Before the Fourier Transform / 3.11:
Data Manipulation After the Fourier Transform / 3.12:
Carbon-13 ( 13 C) NMR Spectroscopy / 4:
Sensitivity of 13 C / 4.1:
Splitting of 13 C Signals / 4.2:
Decoupling / 4.3:
Heteronuclear Decoupling / 4.4:
H Decoupled 13C Spectra
Decoupling Hardware / 4.5:
Decoupling Software: Parameters / 4.6:
The Nuclear Overhauser Effect (NOE) / 4.7:
Heteronuclear Decoupler Modes / 4.8:
NMR Relaxation-Inversion-Recovery and the Nuclear Overhauser Effect (NOE) / 5:
The Vector Model / 5.1:
One Spin in a Magnetic Field / 5.2:
A Large Population of Identical Spins: Net Magnetization / 5.3:
Coherence: Net Magnetization in the x-y Plane / 5.4:
Relaxation / 5.5:
Summary of the Vector Model / 5.6:
Molecular Tumbling and NMR Relaxation / 5.7:
Inversion-Recovery: Measurement of T 1 Values / 5.8:
Continuous-Wave Low-Power Irradiation of One Resonance / 5.9:
Homonuclear Decoupling / 5.10:
Presaturation of Solvent Resonance / 5.11:
The Homonuclear Nuclear Overhauser Effect (NOE) / 5.12:
Summary of the Nuclear Overhauser Effect / 5.13:
The Spin Echo and the Attached Proton Test (APT) / 6:
The Rotating Frame of Reference / 6.1:
The Radio Frequency (RF) Pulse / 6.2:
The Effect of RF Pulses / 6.3:
Quadrature Detection, Phase Cycling, and the Receiver Phase / 6.4:
Chemical Shift Evolution / 6.5:
Scalar (J) Coupling Evolution / 6.6:
Examples of J-coupling and Chemical Shift Evolution / 6.7:
The Attached Proton Test (APT) / 6.8:
The Spin Echo / 6.9:
The Heteronuclear Spin Echo: Controlling J-Coupling Evolution and Chemical Shift Evolution / 6.10:
Coherence Transfer: INEPT and DEPT / 7:
Net Magnetization / 7.1:
Magnetization Transfer / 7.2:
The Product Operator Formalism: Introduction / 7.3:
Single Spin Product Operators: Chemical Shift Evolution / 7.4:
Two-Spin Operators: J-coupling Evolution and Antiphase Coherence / 7.5:
The Effect of RF Pulses on Product Operators / 7.6:
INEPT and the Transfer of Magnetization from 1 H to 13 C / 7.7:
Selective Population Transfer (SPT) as a Way of Understanding INEPT Coherence Transfer / 7.8:
Phase Cycling in INEPT / 7.9:
Intermediate States in Coherence Transfer / 7.10:
Zero- and Double-Quantum Operators / 7.11:
Summary of Two-Spin Operators / 7.12:
Refocused INEPT: Adding Spectral Editing / 7.13:
DEPT: Distortionles / 7.14:
Preface
Acknowledgments
Fundamentalsof NMR Spectroscopy in Liquids / 1:
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電子ブック

EB
editors, Robin K. Harris, Roderick E. Wasylishen, Melinda J. Duer
出版情報: [Ann Arbor, Mich.] : ProQuest Ebook Central, [20--]  1 online resource (xvi, 504 p.)
シリーズ名: EMR handbooks
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3.

電子ブック

EB
edited by Kurt Wüthrich
出版情報: World Scientific  1 online resource (xiv, 250 p.)
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4.

電子ブック

EB
edited by Jens Anders and Jan G. Korvink
出版情報: [Hoboken, N.J.] : Wiley Online Library, 2018  1 online resource (xv, 429 p.)
シリーズ名: Advanced micro & nanosystems ;
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5.

電子ブック

EB
Sławomir Szymański, Piotr Bernatowicz
出版情報: Springer  1 online resource (xi, 402 p.)
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6.

電子ブック

EB
edited by John L. Markley, Stanley J. Opella
出版情報: Oxford University Press  1 online resource
シリーズ名: Oxford scholarship online ;
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Introduction
Acknowledgments
Foreword / R.R. Ernst
The Founders Medal
History of Biological NMR Spectroscopy / Section 1:
Simple Insights from the Beginnings of Magnetic Resonance in Molecular Biology / O. JardetzkyChapter 1:
Choice of Problems in the Early Days of Biological NMR Spectroscopy / M. CohnChapter 2:
Early Days of Biochemical NMR / R.G. ShulmanChapter 3:
William D. Phillips Memorial Lecture / J.J.H. AckermanChapter 4:
Protein Structural Studies / Section 2:
Flexibility and Function of the Escherichia coli trp Repressor / M.R. GrykChapter 5:
Heteronuclear Strategies for the Assignment of Larger protein/DNA complexes: Application to the 37 kDa trp Repressor-Operator Complex / M.J. Revington ; W. Lee ; C.H. ArrowsmithChapter 6:
Design of Novel Hemoglobins / C. Ho ; H.-W. KimChapter 7:
The Role of NMR Spectroscopy in Understanding How Proteins Fold / C.M. DobsonChapter 8:
NMR Approaches To Understanding Protein Specificity / G.C.K. Roberts ; L.-Y. Lian ; I.L. Barsukov ; S. Modi ; W.U. PrimroseChapter 9:
NMR and Mutagenesis Investigations of a Model Cis:Trans Peptide Isomerization Reaction: Xaa[superscript 116]-Pro[superscript 117] of Staphylococcal Nuclease and its Role in Protein Stability and Folding / A.P. Hinck ; W.F. Walkenhorst ; D.M. Truckses ; J.L. MarkleyChapter 10:
A Solid-State NMR Approach to Structure Determination of Membrane Associated Peptides and Proteins / S.J. Opella ; L.E. Chirlian ; B. BechingerChapter 11:
NMR Approaches to the Heat-, Cold-, and Pressure Induced Unfolding of Proteins / K. Akasaka ; T. Yamaguchi ; H. Yamada ; Y. Kamatari ; T. KonnoChapter 12:
Multidimensional NMR Investigation of the Neurotoxic Peptide Mastoparan in the Absence and Presence of Calmodulin / F. Mari ; X. Xie ; J.H. Simpson ; D.J. NelsonChapter 13:
NMR of Larger Proteins: An Approach to the Structural Analyses of Antibody / Y. ArataChapter 14:
Selective Chemical Deuteration of Aromatic Amino Acids: A Retrospective / K.S. Matthews ; R. MatthewsChapter 15:
The Interaction of Antigens and Superantigens with the Human Class II Major Histocompatibility Complex Molecule HLA-DR1 / T. JardetzkyChapter 16:
Chorismate Mutase, Essentially a Template Enzyme / W.N. Lipscomb ; Y.M. Chook ; H. KeChapter 17:
Nucleic Acids / Section 3:
Computing the Structure of Large Complexes: Modeling the 16S Ribosomal RNA / R. Chen ; D. Fink ; R.B. AltmanChapter 18:
Design and Characterization of New Sequence Specific DNA Ligands / D. WemmerChapter 19:
Determination by [superscript 1]H NMR of a Slow Conformational Transition and Hydration Change in the Consensus TATAAT Pribnow Box / C. Milhe ; A. Lane ; J.-F. LefevreChapter 20:
In vivo Spectroscopy / Section 4:
Clinicians Need Localized Proton MRS of the Brain in the Management of HIV-Related Encephalopathies / P.J. Cozzone ; J. Vion-Dury ; S. Confort-Gouny ; F. Nicoli ; A.-M. Salvan ; S. LamoureuxChapter 21:
Nuclear Magnetic Resonance Spectroscopy Studies of Cancer Cell Metabolism / O. Kaplan ; J.S. CohenChapter 22:
Ex Vivo Multinuclear NMR Spectroscopy of Perfused, Respiring Rat Brain Slices: Model Studies of Hypoxia, Ischemia, and Excitotoxicity" / L. Litt ; M.T. Espanol ; Y. Xu ; Y. Cohen ; L.-H. Chang ; P.R. Weinstein ; P.H. Chan ; T.L. JamesChapter 23:
Index
Introduction
Acknowledgments
Foreword / R.R. Ernst
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EB
E.D. Goddard, symposium chairman
出版情報: [S.l.] : ACS Publications  1 online resource (ix, 308 p.)
シリーズ名: Advances in chemistry series ; 84
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8.

電子ブック

EB
W.M. Meier and J.B. Uytterhoeven, editors
出版情報: [S.l.] : ACS Publications  1 online resource (xiii, 634 p.)
シリーズ名: Advances in chemistry series ; 121
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9.

電子ブック

EB
Clara D. Craver, editor, Theodore Provder, editor
出版情報: [S.l.] : ACS Publications  1 online resource (xx, 512 p.)
シリーズ名: Advances in chemistry series ; 227
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Polymer Separation by Thermal
Field-Flow Fractionation: High-Speed Power
Programming Determination of Long-Chain Branching
Distributions of Polyethylenes Automation of High-Temperature Gel Permeation
Chromatography Through the Use of Laboratory Robotics
Characterization of Synthetic Charge-Containing Polymers by Gel Electrophoresis
Particle-Size Distribution by Zero-Angle Depolarized Light
Scattering Latex Particle-Size Distribution from Turbidimetry Using a Combination of Regularization
Techniques and General Cross Validation On-Line
Particle-Size Determination During Latex
Production Using Dynamic Light
Scattering Pressure Bonding and Coherency of Plastic and Fragmentary
Materials Glass Transition Temp as Parameter for Monitoring
Isothermal Cure of Amine-Cured Epoxy System
Characterization of Polymers by Thermal
Stimulated Current and Relaxation Map Analysis
Spectroscopy Thermally Stimulated Creep for the Study of Copolymers and Blends Analysis of Glass
Transition Temperature, Conversion, and Viscosity During Epoxy Resin Curing
Modeling Rheological and Dielectric Properties
During Thermoset Cure In Situ Monitoring of Chemical and Rheological Changes During
Cure in Resin-Transfer Molding Epoxy-Dinorbornene
Spiro Orthocarbonate System by FTIR and Dynamic
Mechanical Spectroscopy Rheokinetic
Measurements of Step- and Chain-Addition Polymerizations
Probing Polymer Structures by Photoacoustic FTIR Spectroscopy
Characterization of Oriented Surfaces by Polarized
Refracometry and Polarized ATR Techniques
IR Studies on Grafting Reactions of Poly(vinyl alcohol)
Development of FTIR Methodology for Evolved Gas Analysis
Simultaneous Differential Scanning
Calorimetry and IR Spectroscopy
Characterization of Crystalline
Polymers by Raman Spectroscopy and Differential
Scanning Calorimetry Free-Volume-Dependent
Fluorescence Probes of Physical Aging in Polymers Solid-State NMR, DSC, and X-ray Difraction
Studies of Polymer Structures, Conformations, Dynamics, and Phase Transitions
Recent Applications of Small-Angle
Neutron Scattering to Multicomponent
Polymer Systems Gels and Foams from Ultra-High-Molecular-Weight Polyethylene
Polymer Separation by Thermal
Field-Flow Fractionation: High-Speed Power
Programming Determination of Long-Chain Branching
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電子ブック

EB
Horacio E. Bergna, editor
出版情報: [S.l.] : ACS Publications  1 online resource (xvii, 695 p.)
シリーズ名: Advances in chemistry series ; 234
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Colloid Chemistry of Silica: An Overview / H.E. Bergna
Silica Nucleation, Polymerization, and Growth: Preparation of Monodispersed Sols / A. Yoshida
The Formation and Interfacial Structure of Silica Sols / J.D. F. Ramsay ; S.W. Swanton ; A. Matsumoto ; D.G. C. Goberdhan
Synthesis and Characterization of Colloidal Model Particles Made from Organoalkoxysilanes / A. van Blaaderen ; A. Vrij
Synthesis of Nanometer-Sized Silica by Controlled Hydrolysis in Reverse Micellar Systems / F.J. Arriagada ; K. Osseo-Asare
Formation of Silica Gels Composed of Micrometer-Sized Particles by the Sol-Gel Method / H. Kozuka ; S. Sakka
Stability of Aqueous Silica Sols / T.W. Healy
The Surface Structure of Amorphous and Crystalline Porous Silicas: Status and Prospects / K.K. Unger
Infrared Study of Chemical and H-D Exchange Probes for Silica Surfaces / B.A. Morrow ; A.J. McFarlan
Fourier Transform Infrared and Raman Spectroscopic Study of Silica Surfaces / A. Burneau ; B. Humbert ; O. Barres ; J.P. Gallas ; J.C. Lavalley
Surveying the Silica Gel Surface with Excited States / R. Krasnansky ; J.K. Thomas
Surface Chemistry and Surface Energy of Silica / A.M. Vidal ; E. Papirer
Variable-Temperature Diffuse Reflectance Fourier Transform Infrared Spectroscopic Studies of Amine Desorption from a Siliceous Surface / D.E. Leyden ; K.G. Proctor
Multinuclear NMR Spectroscopy Studies of Silica Surfaces / G.E. Maciel ; C. E. Bronnimann ; R. C. Zeigler ; I-S. Chuang ; D.R. Kinney ; E.A. Keiter
New Separation Methods for Characterizing the Size of Silica Sols / J.J. Kirkland
Characterization of Colloidal and Particulate Silica by Field-Flow Fractionation / J.C. Giddings ; S.K. Ratanathanawongs ; B.N. Barman ; M.H. Moon ; G. Liu ; L. Tjelta ; M.E. Hansen
Interpretation of the Differences between the Pore Size Distributions of Silica Measured by Mercury Intrusion and Nitrogen Adsorption / A.R. Minihan ; D.R. Ward ; W. Whitby
Sol-Gel Processing of Silica / C.J. Brinker
The Chemistry of Hydrolysis and Condensation of Silica Sol-Gel Precursors / B.K. Coltrain ; L.W. Kelts
Chemistry and Properties of Porous Organically Modified Silica / H. Schmidt ; H. Bottner
Evaporation and Surface Tension Effects in Dip Coating / A.J. Hurd
Formation of Uniform Precipitates / C.F. Zukoski ; J.-L. Look ; G.H. Bogush
Development of Silica Gels and Impact of Silica Research on Studies of Other Colloidal Systems / M.G. Sanchez
Industrial Synthetic Silicas in Powder Form / H.K. Ferch
Adsorptive Properties of Porous Silica 505 / M.B. Kenny ; K.S.W. Sing
Silica Gels from Aqueous Silicate Solutions: A Combined 29Si NMR and Small-Angle X-ray Scattering Spectroscopic Study / P.W.J.G. Wijnen ; T.P.M. Beelen ; R. A. van Santen
Surface Chemistry of Silica Coatings of Titania / D.N. Furlong
Dense Silica Coatings on Micro- and Nanoparticles by Deposition of Monosilicic Acid / L.E. Firment ; D.G. Swartzfager
Applications of Colloidal Silica: Past, Present and Future / C.C. Payne
The Uses of Soluble Silica / J.S. Falcone, Jr.
Silicon-Aluminum Interactions and Biology / J.D. Birchall
Preparation and Uses of Silica Gels and Precipitated Silicas / R.E. Patterson
Colloid Chemistry of Silica: Research in the Former Soviet Union / L.T. Zhuravlev
Colloid Chemistry of Silica: An Overview / H.E. Bergna
Silica Nucleation, Polymerization, and Growth: Preparation of Monodispersed Sols / A. Yoshida
The Formation and Interfacial Structure of Silica Sols / J.D. F. Ramsay ; S.W. Swanton ; A. Matsumoto ; D.G. C. Goberdhan
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