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1.

図書

図書
Ralph J.Fessenden, Joan S.Fessenden著 ; 成田吉徳訳
出版情報: 京都 : 化学同人, 1993.10  xi, 556p ; 26cm
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2.

図書

図書
Ralph J. Fessenden, Joan S. Fessenden
出版情報: Boston, Mass. : W. Grant Press, c1982  xvii, 1069 p. ; 26 cm
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3.

図書

図書
Ralph J. Fessenden, Joan S. Fessenden ; with contributions by John A. Landgrebe
出版情報: Pacific Grove, Calif. : Brooks/Cole, c1993  x, 253 p. ; 24 cm
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目次情報: 続きを見る
Preface
Introduction to the Organic Laboratory
Safety in the Laboratory / 1:
The Laboratory Notebook / 2:
Laboratory Equipment / 3:
Crystallization / Technique 1:
Solvents for Crystallization / 1.1:
Steps in Crystallization / 1.2:
Supplemental Procedures / 1.3:
Melting Points / Technique 2:
Characteristics of Melting Points / 2.1:
Melting-Point Apparatus / 2.2:
Steps in Determining a Melting Point / 2.3:
Extraction / 2.4:
Immiscible Liquids / 3.1:
Distribution Coefficients / 3.2:
Extraction Solvents / 3.3:
Chemically Active Extraction / 3.4:
Steps in Extraction / 3.5:
Additional Techniques Used in Extractions / 3.6:
Other Extraction Techniques / 3.7:
Drying Organic Solutions / Technique 4:
Extraction with Aqueous Sodium Chloride / 4.1:
Solid Inoranic Drying Agents / 4.2:
Procedure for Using Solid Inorganic Drying Agents / 4.3:
Azeotropic Drying / 4.4:
Simple Distillation / Technique 5:
Characteristics of Distillation / 5.1:
Steps in a Simple Distillation / 5.2:
Microscale and Semi-Microscale Distillation / 5.3:
Fractional Distillation / Technique 6:
Efficiency of the Fractionation Column / 6.1:
Steps in Fractional Distillation / 6.2:
Microscale Fractional Distillation / 6.3:
Vacuum Distillation / Technique 7:
Boiling Point and Pressure / 7.1:
Apparatus for Simple Vacuum Distillation / 7.2:
Steps in Vacuum Distillation / 7.3:
Steam Distillation / Technique 8:
Characteristics of Steam Distillation / 8.1:
Amount of Water Needed in a Steam Distillation / 8.2:
Apparatus for Steam Distillation / 8.3:
Sublimation / Technique 9:
Atmospheric Sublimation / 9.1:
Vacuum Sublimation / 9.2:
Refractive Index / Technique 10:
Correcting for Temperature Differences / 10.1:
Steps in Using a Refractometer / 10.2:
Column Chromatography / Technique 11:
Gravity Column Chromatography / 11.1:
Flash Chromatography (Macroscale) / 11.2:
Flash Chromatography (Microscale) / 11.3:
High-Performance Liquid Chromatography (HPLC) / 11.4:
Thin-Layer Chromatography / Technique 12:
The R[subscript f] Value / 12.1:
Equipment for TLC / 12.2:
Steps in a TLC Analysis / 12.3:
A Related Technique: Paper Chromatography / 12.4:
Gas Chromatography / Technique 13:
The Gas Chromatography / 13.1:
Steps in a GC Analysis / 13.3:
Problems Encountered in GC / 13.4:
Uses of Gas Chromatograms / 13.5:
Carrying Out Typical Reactions / Technique 14:
Stirring / 14.1:
Heating Reaction Mixtures / 14.2:
Controlling Exothermic Reactions / 14.3:
Adding Reagents to a Reaction Mixture / 14.4:
Excluding Moisture from a Reaction Mixture / 14.5:
Setting Up a Three-Neck Reaction Flask / 14.6:
Hydrogen Halide Gas Traps / 14.7:
Infrared Spectroscopy / Technique 15:
The Infrared Spectrum / 15.1:
Absorption of Infrared Radiation / 15.2:
Interpreting Infrared Spectra / 15.3:
Identifying Types of Compounds / 15.4:
Preparing a Sample for an Infrared Spectrum / 15.5:
Instrumentation / 15.6:
Proton Nuclear Magnetic Resonance Spectroscopy / Technique 16:
The NMR Spectrum / 16.1:
Interpreting NMR Spectra / 16.2:
Use of Deuterium in Proton NMR Spectroscopy / 16.3:
NMR Spectra of Unknowns / 16.4:
The NMR Spectrometer / 16.5:
Preparing Samples for NMR Spectra / 16.6:
The Chemical Literature / Technique 17:
Introduction to the Chemical Literature / 17.1:
Secondary Literature / 17.2:
Primary Literature / 17.3:
Commonly Used Calculations / Appendix I:
Molarity
Normality
Dilutions
Percent Concentrations / 4:
Percent Yields and Theoretical Yields / 5:
Elemental Analyses / Appendix II:
Determining the Empirical Formula
Determining the Molecular Formula
Interpreting the Results of Elemental Analysis
Degree of Unsaturation
Health Hazards of Compounds Used in Organic Chemistry / Appendix III:
Where to Find Chemical Hazard Information
Understanding Health Hazard Warnings
Preface
Introduction to the Organic Laboratory
Safety in the Laboratory / 1:
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