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1.

図書

図書
ジョーゼフ・B・ランバート著 ; 中島健訳
出版情報: 東京 : 青土社, 1999.6  394, 42, xp ; 20cm
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2.

図書

図書
J.B. Lambert [ほか] 著 ; 務台潔, 小林啓二訳
出版情報: 東京 : 東京化学同人, 1979  2冊 ; 22cm
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3.

図書

図書
Joseph B. Lambert, editor
出版情報: Washington, D.C. : American Chemical Society, 1984  xii, 487 p. ; 24 cm
シリーズ名: Advances in chemistry series ; 205
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4.

図書

図書
edited by Joseph B. Lambert and Frank G. Riddell
出版情報: Dordrecht ; Boston : D. Reidel Pub., in cooperation with NATO Scientific Affairs Division  xvi, 548 p. ; 25 cm
シリーズ名: NATO ASI series ; ser. C . Mathematical and physical sciences ; no. 103
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5.

図書

図書
Joseph B. Lambert, Eugene P. Mazzola, Clark D. Ridge
出版情報: Hoboken, NJ : John Wiley & Sons, 2019  xxii, 456 p. ; 25 cm
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目次情報: 続きを見る
Preface to First Edition
Acknowledgments
Preface to Second Edition
Solutions
Symbols
Abbreviations
Introduction / 1:
Magnetic Properties of Nuclei / 1.1:
The Chemical Shift / 1.2:
Excitation and Relaxation / 1.3:
Pulsed Experiments / 1.4:
The Coupling Constant / 1.5:
Quantitation and Complex Splitting / 1.6:
Commonly Studied Nuclides / 1.7:
Dynamic Effects / 1.8:
Spectra of Solids / 1.9:
Problems
Tips on Solving NMR Problems
References
Further Reading
Introductory Experimental Methods / 2:
The Spectrometer / 2.1:
Sample Preparation / 2.2:
Optimizing the Signal / 2.3:
Sample Tube Placement / 2.3.1:
Probe Tuning / 2.3.2:
Field/Frequency Locking / 2.3.3:
Spectrometer Shimming / 2.3.4:
Determination of NMR Spectral-Acquisition Parameters / 2.4:
Number of Data Points / 2.4.1:
Spectral Width / 2.4.2:
Filter Bandwidth / 2.4.3:
Acquisition Time / 2.4.4:
Transmitter Offset / 2.4.5:
Flip Angle / 2.4.6:
Receiver Gain / 2.4.7:
Number of Scans / 2.4.8:
Steady-State Scans / 2.4.9:
Oversampling and Digital Filtration / 2.4.10:
Decoupling for X Nuclei / 2.4.11:
Typical NMR Experiments / 2.4.12:
Determination of NMR Spectral-Processing Parameters / 2.5:
Exponential Weighting / 2.5.1:
Zero Filling / 2.5.2:
FID Truncation and Spectral Artifacts / 2.5.3:
Resolution / 2.5.4:
Determination of NMR Spectra: Spectral Presentation / 2.6:
Signal Phasing and Baseline Correction / 2.6.1:
Zero Referencing / 2.6.2:
Determination of Certain NMR Parameters / 2.6.3:
Chemical Shifts and Coupling Constants / 2.6.3.1:
1H Integration / 2.6.3.2:
Calibrations / 2.7:
Pulse Width (Flip Angle) / 2.7.1:
Decoupler Field Strength / 2.7.2:
Factors That Influence Proton Shifts / 3:
Local Fields / 3.1.1:
Nonlocal Fields / 3.1.2:
Proton Chemical Shifts and Structure / 3.2:
Saturated Aliphatics / 3.2.1:
Alkanes / 3.2.1.1:
Functionalized Alkanes / 3.2.1.2:
Unsaturated Aliphatics / 3.2.2:
Alkynes / 3.2.2.1:
Alkenes / 3.2.2.2:
Aldehydes / 3.2.2.3:
Aromatics / 3.2.3:
Protons on Oxygen and Nitrogen / 3.2.4:
Programs for Empirical Calculations / 3.2.5:
Medium and Isotope Effects / 3.3:
Medium Effects / 3.3.1:
Isotope Effects / 3.3.2:
Factors That Influence Carbon Shifts / 3.4:
Carbon Chemical Shifts and Structure / 3.5:
Acyclic Alkanes / 3.5.1:
Cyclic Alkanes / 3.5.1.2:
Unsaturated Compounds / 3.5.1.3:
Alkynes and Nitriles / 3.5.2.1:
Carbonyl Groups / 3.5.2.3:
Tables of Chemical Shifts / 3.5.4:
Further Tips on Solving NMR Problems
First- and Second-order Spectra / 4:
Chemical and Magnetic Equivalence / 4.2:
Signs and Mechanisms of Coupling / 4.3:
Couplings over One Bond / 4.4:
Geminal Couplings / 4.5:
Vicinal Couplings / 4.6:
Long-range Couplings / 4.7:
¿- ¿ Overlap / 4.7.1:
Zigzag Pathways / 4.7.2:
Through-Space Coupling / 4.7.3:
Spectral Analysis / 4.8:
Second-order Spectra / 4.9:
Deceptive Simplicity / 4.9.1:
Virtual Coupling / 4.9.2:
Shift Reagents / 4.9.3:
Isotope Satellites / 4.9.4:
Tables of Coupling Constants / 4.10:
Further Topics in One-Dimensional NMR Spectroscopy / 5:
Spin-Lattice and Spin-Spin Relaxation / 5.1:
Causes of Relaxation / 5.1.1:
Measurement of Relaxation Time / 5.1.2:
Transverse Relaxation / 5.1.3:
Structural Ramifications / 5.1.4:
Anisotropic Motion / 5.1.5:
Segmental Motion / 5.1.6:
Partially Relaxed Spectra / 5.1.7:
Quadrupolar Relaxation / 5.1.8:
Reactions on the NMR Time Scale / 5.2:
Hindered Rotation / 5.2.1:
Ring Reversal / 5.2.2:
Atomic Inversion / 5.2.3:
Valence Tautomerizations and Bond Shifts / 5.2.4:
Quantification / 5.2.5:
Magnetization Transfer and Spin Locking / 5.2.6:
Multiple Resonance / 5.3:
Spin Decoupling / 5.3.1:
Difference Decoupling / 5.3.2:
Classes of Multiple Resonance Experiments / 5.3.3:
Off-resonance Decoupling / 5.3.4:
The Nuclear Overhauser Effect / 5.4:
Origin / 5.4.1:
Observation / 5.4.2:
Difference NOE / 5.4.3:
Applications / 5.4.4:
Limitations / 5.4.5:
Spectral Editing / 5.5:
The Spin-Echo Experiment / 5.5.1:
The Attached Proton Test / 5.5.2:
The DEPT Sequence / 5.5.3:
Sensitivity Enhancement / 5.6:
The INEPT sequence / 5.6.1:
Refocused INEPT / 5.6.2:
Spectral Editing with Refocused INEPT / 5.6.3:
DEPT Revisited / 5.6.4:
Carbon Connectivity / 5.7:
Phase Cycling, Composite Pulses, and Shaped Pulses / 5.8:
Phase Cycling / 5.8.1:
Composite Pulses / 5.8.2:
Shaped Pulses / 5.8.3:
Two-Dimensional NMR Spectroscooy / 6:
Proton-Proton Correlation Through/Coupling / 6.1:
COSY45 / 6.1.1:
Long-Range COSY (LRCOSY or Delayed COSY) / 6.1.2:
Phase-Sensitive COSY (¿-COSY) / 6.1.3:
Multiple Quantum Filtration / 6.1.4:
TOtal Correlation SpectroscopY (TOCSY) / 6.1.5:
Relayed COSY / 6.1.6:
J-Resolved Spectroscopy / 6.1.7:
COSY for Other Nuclides / 6.1.8:
Proton-Heteronucleus Correlation / 6.2:
HETCOR / 6.2.1:
HMQC / 6.2.2:
BIRD-HMQC / 6.2.3:
HSQC / 6.2.4:
COLOC / 6.2.5:
HMBC / 6.2.6:
Heteronuclear Relay Coherence Transfer / 6.2.7:
Proton-Proton Correlation Through Space or Chemical Exchange / 6.3:
Carbon-Carbon Correlation / 6.4:
Higher Dimensions / 6.5:
Pulsed Field Gradients / 6.6:
Diffusion-Ordered Spectroscopy / 6.7:
Summary of 2D Methods / 6.8:
Advanced Experimental Methods / 7:
Part A: One-Dimensional Techniques / 7.1:
T1 Measurements / 7.1.1:
13C Spectral Editing Experiments / 7.1.2:
The APT Experiment / 7.1.2.1:
The DEPT Experiment / 7.1.2.2:
NOE Experiments / 7.1.3:
The NOE Difference Experiment / 7.1.3.1:
The Double-Pulse, Field-Gradient, Spin-Echo NOE Experiment / 7.1.3.2:
Part B: Two-Dimensional Techniques / 7.2:
Two-Dimensional NMR Data-Acquisition Parameters / 7.2.1:
Number of Time Increments / 7.2.1.1:
Spectral Widths / 7.2.1.3:
Relaxation Delay / 7.2.1.4:
Number of Scans per Time Increment / 7.2.1.8:
Two-Dimensional NMR Data-Processing Parameters / 7.2.1.10:
Weighting Functions / 7.2.2.1:
Digital Resolution / 7.2.2.2:
Linear Prediction / 7.2.2.4:
Two-Dimensional NMR Data Display / 7.2.3:
Phasing and Zero Referencing / 7.2.3.1:
Symmetrization / 7.2.3.2:
Use of Cross Sections in Analysis / 7.2.3.3:
Part C: Two-Dimensional Techniques: The Experiments / 7.3:
Homonuclear Chemical-Shift Correlation Experiments via Scalar / 7.3.1:
Coupling
The COSY Family: COSY-90°, COSY-45°, Long-Range COSY, and DQF-COSY / 7.3.1.1:
The TOCSY Experiment / 7.3.1.2:
Direct Heteronuclear Chemical-Shift Correlation via Scalar Coupling / 7.3.2:
The HMQC Experiment / 7.3.2.1:
The HSQC Experiment / 7.3.2.2:
The HETCOR Experiment / 7.3.2.3:
Indirect Heteronuclear Chemical-Shift Correlation via Scalar Coupling / 7.3.3:
The HMBC Experiment / 7.3.3.1:
The FLOCK Experiment / 7.3.3.2:
The HSQC-TOCSY Experiment / 7.3.3.3:
Homonuclear Chemical-Shift Correlation via Dipolar Coupling / 7.3.4:
The NOESY Experiment / 7.3.4.1:
The ROESY Experiment / 7.3.4.2:
1D and Advanced 2D Experiments / 7.3.5:
The 1D TOCSY Experiment / 7.3.5.1:
The 1D NOESY and ROESY Experiments / 7.3.5.2:
The Multiplicity-Edited HSQC Experiment / 7.3.5.3:
The H2BC Experiment / 7.3.5.4:
Nonuniform Sampling / 7.3.5.5:
Pure Shift NMR / 7.3.5.6:
Covariance NMR / 7.3.5.7:
Pure Shift-Covariance NMR / 7.3.6:
Structural Elucidation: Two Methods / 8:
Part A: Spectral Analysis / 8.1:
1H NMR Data / 8.1.1:
13C NMR Data / 8.1.2:
The COSY Experiment / 8.13:
General Molecular Assembly Strategy / 8.1.6:
A Specific Molecular Assembly Procedure / 8.1.8:
Part B: Computer-Assisted Structure Elucidation / 8.1.9:
CASE Procedures / 8.2.1:
T-2 Toxin / 8.2.2:
Derivation of the NMR Equation / Appendix A:
The Bloch Equations / Appendix B:
Reference
Quantum Mechanical Treatment of the Two-Spin System / Appendix C:
Analysis of Second-Order. Three- and Four-Spin Systems by Inspection / Appendix D:
Relaxation / Appendix E:
Product-Operator Formalism and Coherence-Level Diagrams / Appendix F:
Stereochemical Considerations / Appendix G:
Homotopics Groups / G.1:
Enantiotopic Groups / G.2:
Diastereotopic Groups / G.3:
Index
Preface to First Edition
Acknowledgments
Preface to Second Edition
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