Elementary Crystallography / 1: |
The Crystalline State / 1-1: |
Crystalline and Amorphous Solids / 1-1.1: |
Definition of a Crystal / 1-1.2: |
Characteristics of the Crystalline and Vitreous States / 1-1.3: |
Crystal Geometry / 1-2: |
External Form and Habit of Crystals / 1-2.1: |
Constancy of Interfacial Angles / 1-2.2: |
Symmetry Elements of Crystals / 1-2.3: |
Pseudosymmetry, 13 / 1-2.4: |
Crystallographic Axes / 1-2.5: |
Axial Ratios / 1-2.6: |
The Six Crystal Symmetry Systems / 1-2.7: |
Miller Indices / 1-2.8: |
The Law of Rational Indices / 1-2.9: |
Crystal Forms / 1-2.10: |
Composite Crystals and Twinning / 1-2.11: |
Equation for the Plane (hkl) / 1-2.12: |
Zones and Zone Relationships / 1-2.13: |
Space Lattices / 1-3: |
Historical Introduction / 1-3.1: |
Definition / 1-3.2: |
The Unit Ceil / 1-3.3: |
The 14 Bravais Lattices / 1-3.4: |
Some Crystallographic Implications of Space Lattices / 1-3.5: |
Distance between Neighboring Lattice Planes in the Series (hkl) / 1-3.6: |
The Reciprocal Lattice / 1-3.7: |
Point Groups and Space Groups / 1-4: |
The Point Group or Crystal Symmetry Class / 1-4.1: |
The Space Group / 1-4.2: |
General References |
Specific References |
The Production and Properties of X-rays / 2: |
X-Ray Safety and Protection / 2-1: |
The Production of X-Rays / 2-2: |
The Origin of X-Rays / 2-2.1: |
X-Ray Tubes / 2-2.2: |
Gas tubes / A: |
Hot-cathode tubes / B: |
Modern diffraction tube design / C: |
Cold-cathode diffraction tubes / D: |
High-intensity diffraction tubes / E: |
Microfocus diffraction tubes / F: |
Power Equipment for the Production of X-rays / 2-2.3: |
Commercial X-ray Generators for Diffraction / 2-2.4: |
Isotopic X-ray Sources / 2-2.5: |
Properties of X-Rays and their Measurement / 2-3: |
The X-ray Spectrum of an Element / 2-3.1: |
The continuous x-ray spectrum |
The characteristic x-ray spectrum |
The Precise Determination of X-ray Wavelengths / 2-3.2: |
Absorption of X-rays / 2-3.3: |
Secondary Fluorescent and Scattered X-rays / 2-3.4: |
Refraction of X-rays / 2-3.5: |
Monochromatization of X-radiation / 2-3.6: |
Single filter technique |
Balanced-filter technique |
Crystal monochromator techniques |
Graphite monochromators |
The Photographic Effects of X-rays / 2-3.7: |
Fundamental Principles of X-ray Diffraction / 3: |
Kinematical and Dynamical Diffraction Theory / 3-1: |
The Geometry of Diffraction / 3-2: |
Scattering of X-rays by Electrons and Atoms / 3-2.1: |
Scattering by a Regularly Spaced Row of Atoms / 3-2.2: |
Conditions for Diffraction by a Linear Lattice of Atoms / 3-2.3: |
Diffraction by a Simple Cubic Lattice / 3-2.4: |
Proof that the "Diffracting Plane" is a Lattice Plane / 3-2.5: |
The Bragg Equation / 3-2.6: |
Derivation of the Bragg Equation from the "Reflection" Analogy / 3-2.7: |
The Geometrical Picture of Diffraction in Reciprocal Space / 3-2.8: |
The Intensity of Diffraction / 3-3: |
Perfect and Imperfect Crystals / 3-3.1: |
Primary and Secondary Extinction / 3-3.2: |
Relative and Absolute Intensities / 3-3.3: |
Factors Affecting the Diffraction Intensities / 3-3.4: |
The polarization factor |
The Lorentz and "velocity" factors |
The temperature factor |
The atomic scattering factor |
The structure factor |
The multiplicity factor |
The absorption factor / G: |
Expressions for the Relative Intensity of Diffraction by the Various Techniques / 3-3.5: |
Lattice-Centering and Space-Group Extinctions / 3-3.6: |
Photographic Powder Techniques / 4: |
The Debye-Scherrer Method / 4-1: |
Introduction / 4-1.1: |
Camera Design / 4-1.2: |
General geometry |
Details of camera construction |
Camera support and alignment |
Preparation of the Powder / 4-1.3: |
Mounting the Powder / 4-1.4: |
Making the Exposure / 4-1.5: |
Processing the Film / 4-1.6: |
Parafocusing Methods / 4-2: |
Monochromatic-Pinhole Techniques / 4-3: |
Forward-Reflection Method / 4-3.1: |
Back-Reflection Method / 4-3.2: |
Microcameras and Microbeam Techniques / 4-4: |
High-Temperature Techniques / 4-5: |
Low-Temperature Techniques / 4-6: |
High-Pressure Techniques / 4-7: |
Diffractometric Powder Technique |
Geometry of the Powder Diffractometer / 5-1: |
General Features / 5-1.1: |
Details of the Optical Arrangement / 5-1.2: |
The Seemann-Bohlin Diffractometer / 5-1.3: |
Alignment and Angular Calibration of the Diffractometer / 5-1.4: |
Operations appropriately performed in advance by the manufacturer |
Further internal alignment of the goniometer |
Alignment of the goniometer with respect to the x-ray tube |
Calibration of the O? 2Theta; position |
Calibration of angular registration between 0 and 180? 2Theta; |
Profiles and positions of diffraction maxima / 5-2: |
Convolution Synthesis of Line Profiles / 5-2.1: |
X-ray source, g I |
Flat specimen surface, g II |
Axial divergence, g III |
Specimen transparency, g IV |
Receiving slit, g v |
Comparison of calculated and experimental line profiles |
Displacement and Breadth of Diffraction Maxima / 5-2.2: |
Line position |
Line breadth |
The practical determination of the centroid and variance |
Accurate Determination of Interplanar (d) Spacings / 5-2.3: |
"Routine" Determination of Interplanar (d) Spacings / 5-2.4: |
Electrical Characteristics of the Diffractometer / 5-3: |
General Arrangement of Components / 5-3.1: |
Radiation Detectors (Quantum Counters) / 5-3.2: |
Gas-ionization counters |
Geiger-Muller counters |
Proportional counters |
Scintillation counters |
Solid-state (energy-dispersive) detectors |
Nonlinearity of Detector Response / 5-3.3: |
Monochromatizing Techniques / 5-3.4: |
Pulse-height discrimination and analysis |
Ross balanced filters |
Crystal monochromators |
Choice of Experimental Conditions and Procedures / 5-4: |
Statistical Accuracy of Counter Measurements / 5-4.1: |
The Specimen / 5-4.2: |
Preparation of powders |
Rotation of the specimen |
Preferred orientation and the specimen mount |
High-temperature techniques |
Low-temperature techniques |
Other special specimen techniques |
Transmission Techniques / 5-4.3: |
Continuous-Scan Techniques / 5-4.4: |
Step-Scan Techniques and Automation / 5-4.5: |
The Interpretation of Powder Diffraction Data / 6: |
The Viewing and Precision Measurement of Powder Photographs / 6-1: |
Determination of Interplanar (d) Spacings / 6-2: |
Debye-Scherrer Patterns / 6-2.1: |
Monochromatic-Pinhole (Flat-Film) Patterns / 6-2.2: |
Indexing Cubic Powder Patterns / 6-3: |
Reciprocal-Lattice Picture of Diffraction by a Cubic Powder / 6-3.1: |
Indexing a Cubic Pattern by sin 2 Theta Ratios / 6-3.2: |
Determination of the Unit-Cell Dimension a / 6-3.3: |
Indexing a Cubic Pattern When a Is Known / 6-3.4: |
Determination of Lattice Type / 6-4: |
Indexing Noncubic Powder Patterns / 6-5: |
Indexing Noncubic Patterns When the Unit-Cell Dimensions are Known / 6-5.1: |
Graphical Methods of Indexing / 6-5.2: |
Analytical Methods of Indexing: Tetragonal, Hexagonal, and Orthorhombic Patterns / 6-5.3: |
Analytical Methods of Indexing: Monoclinic and Triclinic Patterns / 6-5.4: |
Automated Computing Procedures for Indexing Powder Patterns / 6-6: |
Programs for Patterns of Orthorhombic and Higher Symmetry / 6-6.1: |
Programs for Patterns of Low Symmetry / 6-6.2: |
The Measurement of Intensities from Photographic Blackening / 6-7: |
Preparation of a Graded Intensity Scale / 6-7.1: |
Visual Estimation of Intensities / 6-7.3: |
Photometer Techniques / 6-7.4: |
The Measurement of Intensities with the X-Ray Diffractometer / 6-8: |
Putting Intensities on an Absolute Scale / 6-9: |
Special Scattering and Diffraction Effects / 6-10: |
Background Effects / 6-10.1: |
Background due to lattice imperfections |
Background due to general radiation |
Absorption discontinuities |
Air scatter |
Secondary fluorescence radiation |
Reflections of Unusual Char / 6-10.2: |
Elementary Crystallography / 1: |
The Crystalline State / 1-1: |
Crystalline and Amorphous Solids / 1-1.1: |